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A stereoselective hydroxylation and enantioselective dehalogenation cascade reaction was developed for the synthesis of optically active beta-haloalcohols from halohydrocarbons. This cascade system employed P450 and halohydrin dehalogenase as two compatible biocatalysts, allowing a straightforward, greener and efficient access to beta-halohydrins with excellent enantioselectivities (98-99%).
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