COA of Formula: C12H12N2. The reaction of aromatic heterocyclic molecules with protons is called protonation. Aromatic heterocycles are more basic than benzene due to the participation of heteroatoms. Compound: 5,5′-Dimethyl-2,2′-bipyridine, is researched, Molecular C12H12N2, CAS is 1762-34-1, about Dual Cobalt and Photoredox Catalysis Enabled Redox-Neutral Annulation of 2-Propynolphenols. Author is Zhu, Yao; He, Yong-Qin; Tian, Wan-Fa; Wang, Mei; Zhou, Zhao-Zhao; Song, Xian-Rong; Ding, Hai-Xin; Xiao, Qiang.
A hydroxyl-assisted, organophotoredox/cobalt dual catalyzed annulation of 2-propynolphenols I [R1 = H, R2 = H, F, Cl, Br, MeO2C, Me; R1 = Cl, R2 = H; R1 = R2 = F; R3 = R4 = Me, Ph, 4-FC6H4, 3-F3CC6H4, etc.; R3 = Ph, R4 = Me, 4-ClC6H4, 2-FC6H4, 4-F3CC6H4, 2-thienyl, etc.; R3 = 4-FC6H4, R4 = 4-MeOC6H4; R3R4 = (CH2)5] to form 2-(hydroxymethyl)benzo[b]furans II has been developed by employing 1,2,3,5-tetrakis(carbazol-9-yl)-4,6-dicyanobenzene (4CzIPN) as photosensitizer and CoCl2(PPh3)2/5,5′-dimethyl-2,2′-bipyridine as cobalt catalytic precursor. Various substrates and functional groups were tolerated. The practical applications of this reaction were further demonstrated by enlarged gram-scale and various derivations for complex heterocycles. Primary mechanistic studies suggested the involvement of cobalt-hydride mediated hydrogen atom transfer (HAT) process.
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